Electrochemistry Open LessonsSustainable Electrochemical Science & Technology, BRIN

Tools

Sensor calibration

Fit a calibration line, then get sensitivity, linear range, LOD and LOQ, and check recovery and RSD in real samples. The background is in Lesson 4.2.

Sources

  1. J. Mocak, A. M. Bond, S. Mitchell, G. Scollary, A statistical overview of standard (IUPAC and ACS) and new procedures for determining the limits of detection and quantification, application to voltammetric and stripping techniques, Pure Appl. Chem. 69 (1997) 297–328. IUPAC page
  2. International Council for Harmonisation, Guideline Q2(R2), Validation of analytical procedures, 2023.

These tools are for learning and quick checks. Keep the raw data and the full calculation for any paper, and state every assumption in the methods.